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Method to synthesize lanthanide fluoride materials from lanthanide fluorinated alkoxides

United States Patent Application

*** PATENT GRANTED ***
20160229773
9,981,893
A1
View the Complete Application at the US Patent & Trademark Office
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Lanthanide fluorinated alkoxide derivatives can be synthesized from the alcoholysis reaction of the lanthanide bis-trimethylsilyl amide and an excess amount of hexafluoro iso-propanol. Nanoparticles can be formed from the lanthanide fluorinated alkoxide derivatives by a solvothermal or solution precipitation process.
Boyle, Timothy J. (Albuquerque, NM)
15/ 010,899
January 29, 2016
STATEMENT OF GOVERNMENT INTEREST [0002] This invention was made with Government support under contract no. DE-AC04-94AL85000 awarded by the U. S. Department of Energy to Sandia Corporation. The Government has certain rights in the invention.