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Production of Nanocrystalline Metal Powders via Combustion Reaction Synthesis

United States Patent Application

*** PATENT GRANTED ***
20110194970
9,802,834
A1
View the Complete Application at the US Patent & Trademark Office
Pacific Northwest National Laboratory - Visit the Technology Commercialization Program Website
Nanocrystalline metal powders comprising tungsten, molybdenum, rhenium or niobium can be synthesized using a combustion reaction. Methods for synthesizing the nanocrystalline metal powders are characterized by forming a combustion synthesis solution by dissolving in water an oxidizer, a fuel, and a base-soluble, ammonium precursor of tungsten, molybdenum, rhenium, or niobium in amounts that yield a soichiometric burn when combusted. The combustion synthesis solution is then heated to a temperature sufficient to substantially remove water and to initiate a self-sustaining combustion reaction. The resulting powder can be subsequently reduced to metal form by heating in a reducing gas environment.
Frye, John G. (Richland, WA), Weil, Kenneth Scott (Richland, WA), Lavender, Curt A. (Richland, WA), Kim, Jin Yong (Richland, WA)
BATTELLE MEMORIAL INSTITUTE (Richland WA)
12/ 700,923
February 5, 2010
STATEMENT REGARDING FEDERALLY SPONSORED RESEARCH OR DEVELOPMENT [0001] This invention was made with Government support under Contract DE-AC0576RL01830 awarded by the U.S. Department of Energy. The Government has certain rights in the invention.